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Reagent control over the composition of mixed metal oxide nanoparticles

Alvin W. Orbaek, Lauren Morrow, Samuel J. Maguire-Boyle, Andrew Barron Orcid Logo

Journal of Experimental Nanoscience, Volume: 10, Issue: 5, Pages: 324 - 349

Swansea University Author: Andrew Barron Orcid Logo

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DOI (Published version): 10.1080/17458080.2013.832422

Abstract

Binary and ternary metal-oxide nanoparticles have been prepared by thermal decomposition of the appropriate metal (M = Fe, Mn, Pd, Cu, Al, Gd) compounds in the presence of oleic acid, oleylamine, and 1,2-hexadecanediol as an accelerating agent. The metal percentage and the particle size were investi...

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Published in: Journal of Experimental Nanoscience
Published: 2013
URI: https://cronfa.swan.ac.uk/Record/cronfa22194
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first_indexed 2015-06-27T02:06:57Z
last_indexed 2018-02-09T05:00:25Z
id cronfa22194
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spelling 2015-06-26T15:47:15.3437870 v2 22194 2015-06-26 Reagent control over the composition of mixed metal oxide nanoparticles 92e452f20936d688d36f91c78574241d 0000-0002-2018-8288 Andrew Barron Andrew Barron true false 2015-06-26 CHEG Binary and ternary metal-oxide nanoparticles have been prepared by thermal decomposition of the appropriate metal (M = Fe, Mn, Pd, Cu, Al, Gd) compounds in the presence of oleic acid, oleylamine, and 1,2-hexadecanediol as an accelerating agent. The metal percentage and the particle size were investigated as a function of the starting composition. The NP composition is controlled by the relative reaction rates of the particular precursors, such that prediction of NP composition from reagent ratios is not straightforward. An understanding of reaction rate limitations allows for alternative synthesis to be developed. Journal Article Journal of Experimental Nanoscience 10 5 324 349 26 9 2013 2013-09-26 10.1080/17458080.2013.832422 COLLEGE NANME Chemical Engineering COLLEGE CODE CHEG Swansea University 2015-06-26T15:47:15.3437870 2015-06-26T15:47:15.3437870 Faculty of Science and Engineering School of Engineering and Applied Sciences - Chemical Engineering Alvin W. Orbaek 1 Lauren Morrow 2 Samuel J. Maguire-Boyle 3 Andrew Barron 0000-0002-2018-8288 4
title Reagent control over the composition of mixed metal oxide nanoparticles
spellingShingle Reagent control over the composition of mixed metal oxide nanoparticles
Andrew Barron
title_short Reagent control over the composition of mixed metal oxide nanoparticles
title_full Reagent control over the composition of mixed metal oxide nanoparticles
title_fullStr Reagent control over the composition of mixed metal oxide nanoparticles
title_full_unstemmed Reagent control over the composition of mixed metal oxide nanoparticles
title_sort Reagent control over the composition of mixed metal oxide nanoparticles
author_id_str_mv 92e452f20936d688d36f91c78574241d
author_id_fullname_str_mv 92e452f20936d688d36f91c78574241d_***_Andrew Barron
author Andrew Barron
author2 Alvin W. Orbaek
Lauren Morrow
Samuel J. Maguire-Boyle
Andrew Barron
format Journal article
container_title Journal of Experimental Nanoscience
container_volume 10
container_issue 5
container_start_page 324
publishDate 2013
institution Swansea University
doi_str_mv 10.1080/17458080.2013.832422
college_str Faculty of Science and Engineering
hierarchytype
hierarchy_top_id facultyofscienceandengineering
hierarchy_top_title Faculty of Science and Engineering
hierarchy_parent_id facultyofscienceandengineering
hierarchy_parent_title Faculty of Science and Engineering
department_str School of Engineering and Applied Sciences - Chemical Engineering{{{_:::_}}}Faculty of Science and Engineering{{{_:::_}}}School of Engineering and Applied Sciences - Chemical Engineering
document_store_str 0
active_str 0
description Binary and ternary metal-oxide nanoparticles have been prepared by thermal decomposition of the appropriate metal (M = Fe, Mn, Pd, Cu, Al, Gd) compounds in the presence of oleic acid, oleylamine, and 1,2-hexadecanediol as an accelerating agent. The metal percentage and the particle size were investigated as a function of the starting composition. The NP composition is controlled by the relative reaction rates of the particular precursors, such that prediction of NP composition from reagent ratios is not straightforward. An understanding of reaction rate limitations allows for alternative synthesis to be developed.
published_date 2013-09-26T03:26:24Z
_version_ 1763750953108897792
score 10.998116

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