Journal article 504 views
Aging of the reaction mixture as a tool to modulate the crystallite size of UiO-66 into the low nanometer range
Marco Taddei 
,
Kim Corinna Dümbgen,
Jeroen Anton van Bokhoven,
Marco Ranocchiari
,
Kim Corinna Dümbgen,
Jeroen Anton van Bokhoven,
Marco Ranocchiari
Chemical Communications, Volume: 52, Issue: 38, Pages: 6411 - 6414
Swansea University Author:
Marco Taddei
Full text not available from this repository: check for access using links below.
DOI (Published version): 10.1039/c6cc02517j
Abstract
Nanosized UiO-66 with an unprecedented crystallite size of 10 nm was synthesized by exploiting controlled aging of stock solutions of Zr4+ in N,N-dimethylformamide in the presence of variable amounts of water and acetic acid prior to the addition of the ligand. The yield of the synthesis is not affe...
| Published in: | Chemical Communications |
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| ISSN: | 1359-7345 1364-548X |
| Published: |
Royal Society of Chemistry (RSC)
2016
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| Online Access: |
Check full text
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| URI: | https://cronfa.swan.ac.uk/Record/cronfa32744 |
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| Abstract: |
Nanosized UiO-66 with an unprecedented crystallite size of 10 nm was synthesized by exploiting controlled aging of stock solutions of Zr4+ in N,N-dimethylformamide in the presence of variable amounts of water and acetic acid prior to the addition of the ligand. The yield of the synthesis is not affected, affording high conversion of the starting reagents into the product. |
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| College: |
Faculty of Science and Engineering |
| Issue: |
38 |
| Start Page: |
6411 |
| End Page: |
6414 |