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Performance comparison of 2D nickel phosphate nanoparticles prepared via sonochemical and microwave-assisted hydrothermal routes for supercapattery

Norshahirah Mohamad Saidi, Artiqah Khairudin, Lijie Li Orcid Logo, Muhammad Amirul Aizat Mohd Abdah, Ong Gerard, Yee Seng Tan, Mohammad Khalid, Fayaz Khan, Muhammad Norhaffis Mustafa, Arshid Numan

Journal of Energy Storage, Volume: 73, Start page: 108846

Swansea University Author: Lijie Li Orcid Logo

  • Accepted Manuscript under embargo until: 31st August 2024

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DOI (Published version): 10.1016/j.est.2023.108846

Abstract

Metal phosphates are broadly applied in electrochemical energy storage applications because of their abundance in nature, cost-effectiveness, and excellent electrochemical performance. Herein, we compare the performance of nickel phosphate (Ni3(PO4)2) prepared through sonochemical and microwave-assi...

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Published in: Journal of Energy Storage
ISSN: 2352-152X
Published: Elsevier BV 2023
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URI: https://cronfa.swan.ac.uk/Record/cronfa64306
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spelling v2 64306 2023-09-01 Performance comparison of 2D nickel phosphate nanoparticles prepared via sonochemical and microwave-assisted hydrothermal routes for supercapattery ed2c658b77679a28e4c1dcf95af06bd6 0000-0003-4630-7692 Lijie Li Lijie Li true false 2023-09-01 EEEG Metal phosphates are broadly applied in electrochemical energy storage applications because of their abundance in nature, cost-effectiveness, and excellent electrochemical performance. Herein, we compare the performance of nickel phosphate (Ni3(PO4)2) prepared through sonochemical and microwave-assisted hydrothermal reaction (MW) synthesis routes for supercapattery. These methods are efficient, rapid, and facile, yielding a high quantity of nanoparticles. Field Emission Scanning Electron Microscopy reveals that Ni3(PO4)2 nanoparticles synthesized via the MW method are smaller than those produced via the sonochemical method. X-ray diffraction analysis confirmed that the MW method, followed by calcination at 200 °C for 3 h (NiPO4-MWB sample), produces amorphous nanoparticles, providing more exposure to redox-active sites. This work demonstrates that the NiPO4-MWB sample exhibits the highest specific capacity of 256.54C g−1 at a current density of 1 A g−1 compared to its counterpart electrode prepared via the sonochemical. A device fabricated using NiPO4-MWB//activated carbon (AC) delivered an energy density of 10.33 Wh kg−1 at a power density of 750 W kg−1, retaining 99.42 % of its capacity after 5000 cycles. The notable capacity retention makes it an attractive candidate for supercapattery electrodes. These findings suggest that MW synthesis can be used for the rapid production of tailored nanoparticles for electrochemical energy storage applications. Journal Article Journal of Energy Storage 73 108846 Elsevier BV 2352-152X Nickel phosphate, Sonochemical, Microwave hydrothermal, Supercapattery 1 12 2023 2023-12-01 10.1016/j.est.2023.108846 http://dx.doi.org/10.1016/j.est.2023.108846 COLLEGE NANME Electronic and Electrical Engineering COLLEGE CODE EEEG Swansea University Not Required The authors would like to acknowledge the funding support under Sunway University Internal Grant Scheme (GRTIN-IGS-GAMRG[S]-13-2022). 2023-10-27T14:43:12.5606118 2023-09-01T14:46:39.1810770 Faculty of Science and Engineering School of Aerospace, Civil, Electrical, General and Mechanical Engineering - Electronic and Electrical Engineering Norshahirah Mohamad Saidi 1 Artiqah Khairudin 2 Lijie Li 0000-0003-4630-7692 3 Muhammad Amirul Aizat Mohd Abdah 4 Ong Gerard 5 Yee Seng Tan 6 Mohammad Khalid 7 Fayaz Khan 8 Muhammad Norhaffis Mustafa 9 Arshid Numan 10 Under embargo Under embargo 2023-09-01T14:50:31.1697140 Output 1351867 application/pdf Accepted Manuscript true 2024-08-31T00:00:00.0000000 false eng
title Performance comparison of 2D nickel phosphate nanoparticles prepared via sonochemical and microwave-assisted hydrothermal routes for supercapattery
spellingShingle Performance comparison of 2D nickel phosphate nanoparticles prepared via sonochemical and microwave-assisted hydrothermal routes for supercapattery
Lijie Li
title_short Performance comparison of 2D nickel phosphate nanoparticles prepared via sonochemical and microwave-assisted hydrothermal routes for supercapattery
title_full Performance comparison of 2D nickel phosphate nanoparticles prepared via sonochemical and microwave-assisted hydrothermal routes for supercapattery
title_fullStr Performance comparison of 2D nickel phosphate nanoparticles prepared via sonochemical and microwave-assisted hydrothermal routes for supercapattery
title_full_unstemmed Performance comparison of 2D nickel phosphate nanoparticles prepared via sonochemical and microwave-assisted hydrothermal routes for supercapattery
title_sort Performance comparison of 2D nickel phosphate nanoparticles prepared via sonochemical and microwave-assisted hydrothermal routes for supercapattery
author_id_str_mv ed2c658b77679a28e4c1dcf95af06bd6
author_id_fullname_str_mv ed2c658b77679a28e4c1dcf95af06bd6_***_Lijie Li
author Lijie Li
author2 Norshahirah Mohamad Saidi
Artiqah Khairudin
Lijie Li
Muhammad Amirul Aizat Mohd Abdah
Ong Gerard
Yee Seng Tan
Mohammad Khalid
Fayaz Khan
Muhammad Norhaffis Mustafa
Arshid Numan
format Journal article
container_title Journal of Energy Storage
container_volume 73
container_start_page 108846
publishDate 2023
institution Swansea University
issn 2352-152X
doi_str_mv 10.1016/j.est.2023.108846
publisher Elsevier BV
college_str Faculty of Science and Engineering
hierarchytype
hierarchy_top_id facultyofscienceandengineering
hierarchy_top_title Faculty of Science and Engineering
hierarchy_parent_id facultyofscienceandengineering
hierarchy_parent_title Faculty of Science and Engineering
department_str School of Aerospace, Civil, Electrical, General and Mechanical Engineering - Electronic and Electrical Engineering{{{_:::_}}}Faculty of Science and Engineering{{{_:::_}}}School of Aerospace, Civil, Electrical, General and Mechanical Engineering - Electronic and Electrical Engineering
url http://dx.doi.org/10.1016/j.est.2023.108846
document_store_str 0
active_str 0
description Metal phosphates are broadly applied in electrochemical energy storage applications because of their abundance in nature, cost-effectiveness, and excellent electrochemical performance. Herein, we compare the performance of nickel phosphate (Ni3(PO4)2) prepared through sonochemical and microwave-assisted hydrothermal reaction (MW) synthesis routes for supercapattery. These methods are efficient, rapid, and facile, yielding a high quantity of nanoparticles. Field Emission Scanning Electron Microscopy reveals that Ni3(PO4)2 nanoparticles synthesized via the MW method are smaller than those produced via the sonochemical method. X-ray diffraction analysis confirmed that the MW method, followed by calcination at 200 °C for 3 h (NiPO4-MWB sample), produces amorphous nanoparticles, providing more exposure to redox-active sites. This work demonstrates that the NiPO4-MWB sample exhibits the highest specific capacity of 256.54C g−1 at a current density of 1 A g−1 compared to its counterpart electrode prepared via the sonochemical. A device fabricated using NiPO4-MWB//activated carbon (AC) delivered an energy density of 10.33 Wh kg−1 at a power density of 750 W kg−1, retaining 99.42 % of its capacity after 5000 cycles. The notable capacity retention makes it an attractive candidate for supercapattery electrodes. These findings suggest that MW synthesis can be used for the rapid production of tailored nanoparticles for electrochemical energy storage applications.
published_date 2023-12-01T14:43:11Z
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