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The Importance of Rubber Compounding Approach in Damage Evolution and Fatigue Performance of Carbon Nanotubes Doped Natural Rubber

Ali Esmaeili, DEEPAK GEORGE, Thomas Lake Orcid Logo, Lewis Tunnicliffe, Ian Masters Orcid Logo, Mokarram Hossain Orcid Logo

Fatigue & Fracture of Engineering Materials & Structures

Swansea University Authors: Ali Esmaeili, DEEPAK GEORGE, Thomas Lake Orcid Logo, Ian Masters Orcid Logo, Mokarram Hossain Orcid Logo

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DOI (Published version): 10.1111/ffe.70065

Abstract

This study was aimed to investigate the fatigue life of carbon nanotubes (CNTs) filled natural rubbers (NR) prepared by two different compounding techniques, including wet and dry methods. This was done to correlate the presence of defects to fatigue performance and to identify the optimum dispersio...

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Published in: Fatigue & Fracture of Engineering Materials & Structures
ISSN: 8756-758X 1460-2695
Published: Wiley 2025
Online Access: Check full text

URI: https://cronfa.swan.ac.uk/Record/cronfa70163
Abstract: This study was aimed to investigate the fatigue life of carbon nanotubes (CNTs) filled natural rubbers (NR) prepared by two different compounding techniques, including wet and dry methods. This was done to correlate the presence of defects to fatigue performance and to identify the optimum dispersion approach for CNTs/NR. The wet approach possessed a higher number of large defects compared to the dry approach, whereas the latter manifested better CNT dispersion. The presence of a higher number of large defects accounted for a significant reduction in the fatigue life in the wet batch with respect to dry samples. The formation of multiple tiny cracks and their further developments via crack shielding and crack coalescence were considered for damage evolution at the macroscale, while the presence of wrenching and river-like patterns was notable at the microscale. Ultimately, the dry approach could be a better compounding technique for CNT dispersion considering its high quasi-static and fatigue properties.
Keywords: carbon nanotubes; compounding technique; damage evolution; defect; fatigue life; natural rubber
College: Faculty of Science and Engineering
Funders: Swansea Bay City Deal and the European Regional Development Fund through the Welsh European Funding Office; EPSRC through the Supergen ORE Hub (EP/S000747/1), who have awarded funding for the Flexible Fund project Submerged biaxial fatigue analysis for Flexible membrane Wave Energy Converters (FF2021-1036); Birla Carbon, USA