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Versatile electrochemical cell for Li/Na-ion batteries and high-throughput setup for combined operando X-ray diffraction and absorption spectroscopy / Jonas Sottmann; Roberto Homs-Regojo; David S. Wragg; Helmer Fjellvåg; Serena Margadonna; Hermann Emerich

Journal of Applied Crystallography, Volume: 49, Issue: 6, Pages: 1972 - 1981

Swansea University Author: Margadonna, Serena

Abstract

A fully operational setup (electrochemical cells, sample changer and interfacing software) that enables combined quasi-simultaneous operando X-ray diffraction (XRD) and absorption (XANES and EXAFS) measurements coupled with electrochemical characterization has been realized for synchrotron based stu...

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Published in: Journal of Applied Crystallography
ISSN: 1600-5767
Published: 2016
Online Access: Check full text

URI: https://cronfa.swan.ac.uk/Record/cronfa31079
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Abstract: A fully operational setup (electrochemical cells, sample changer and interfacing software) that enables combined quasi-simultaneous operando X-ray diffraction (XRD) and absorption (XANES and EXAFS) measurements coupled with electrochemical characterization has been realized for synchrotron based studies. Combined XRD, XANES and EXAFS analysis provides a deep insight into the working mechanisms of electrode materials.
Keywords: in-operando measurements, crystal structure, powder diffraction, electrode materials for secondary batteries, electrochemical cells
College: College of Engineering
Issue: 6
Start Page: 1972
End Page: 1981