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Versatile electrochemical cell for Li/Na-ion batteries and high-throughput setup for combined operando X-ray diffraction and absorption spectroscopy

Jonas Sottmann, Roberto Homs-Regojo, David S. Wragg, Helmer Fjellvåg, Serena Margadonna Orcid Logo, Hermann Emerich

Journal of Applied Crystallography, Volume: 49, Issue: 6, Pages: 1972 - 1981

Swansea University Author: Serena Margadonna Orcid Logo

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DOI (Published version): 10.1107/S160057671601428X

Abstract

A fully operational setup (electrochemical cells, sample changer and interfacing software) that enables combined quasi-simultaneous operando X-ray diffraction (XRD) and absorption (XANES and EXAFS) measurements coupled with electrochemical characterization has been realized for synchrotron based stu...

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Published in: Journal of Applied Crystallography
ISSN: 1600-5767
Published: 2016
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URI: https://cronfa.swan.ac.uk/Record/cronfa31079
first_indexed 2017-05-12T18:56:03Z
last_indexed 2018-04-14T04:19:04Z
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spelling 2018-04-12T11:46:49.9516377 v2 31079 2016-11-15 Versatile electrochemical cell for Li/Na-ion batteries and high-throughput setup for combined operando X-ray diffraction and absorption spectroscopy e31904a10b1b1240b98ab52d9977dfbe 0000-0002-6996-6562 Serena Margadonna Serena Margadonna true false 2016-11-15 EAAS A fully operational setup (electrochemical cells, sample changer and interfacing software) that enables combined quasi-simultaneous operando X-ray diffraction (XRD) and absorption (XANES and EXAFS) measurements coupled with electrochemical characterization has been realized for synchrotron based studies. Combined XRD, XANES and EXAFS analysis provides a deep insight into the working mechanisms of electrode materials. Journal Article Journal of Applied Crystallography 49 6 1972 1981 1600-5767 in-operando measurements, crystal structure, powder diffraction, electrode materials for secondary batteries, electrochemical cells 31 12 2016 2016-12-31 10.1107/S160057671601428X https://doi.org/10.1107/S160057671601428X COLLEGE NANME Engineering and Applied Sciences School COLLEGE CODE EAAS Swansea University 2018-04-12T11:46:49.9516377 2016-11-15T11:11:03.6578925 Faculty of Science and Engineering School of Engineering and Applied Sciences - Chemical Engineering Jonas Sottmann 1 Roberto Homs-Regojo 2 David S. Wragg 3 Helmer Fjellvåg 4 Serena Margadonna 0000-0002-6996-6562 5 Hermann Emerich 6 0031079-11052017155021.pdf JApplCryst-ResearchPaper-InOperandoCell-20160511.pdf 2017-05-11T15:50:21.7330000 Output 2466725 application/pdf Accepted Manuscript true 2017-05-11T00:00:00.0000000 true eng
title Versatile electrochemical cell for Li/Na-ion batteries and high-throughput setup for combined operando X-ray diffraction and absorption spectroscopy
spellingShingle Versatile electrochemical cell for Li/Na-ion batteries and high-throughput setup for combined operando X-ray diffraction and absorption spectroscopy
Serena Margadonna
title_short Versatile electrochemical cell for Li/Na-ion batteries and high-throughput setup for combined operando X-ray diffraction and absorption spectroscopy
title_full Versatile electrochemical cell for Li/Na-ion batteries and high-throughput setup for combined operando X-ray diffraction and absorption spectroscopy
title_fullStr Versatile electrochemical cell for Li/Na-ion batteries and high-throughput setup for combined operando X-ray diffraction and absorption spectroscopy
title_full_unstemmed Versatile electrochemical cell for Li/Na-ion batteries and high-throughput setup for combined operando X-ray diffraction and absorption spectroscopy
title_sort Versatile electrochemical cell for Li/Na-ion batteries and high-throughput setup for combined operando X-ray diffraction and absorption spectroscopy
author_id_str_mv e31904a10b1b1240b98ab52d9977dfbe
author_id_fullname_str_mv e31904a10b1b1240b98ab52d9977dfbe_***_Serena Margadonna
author Serena Margadonna
author2 Jonas Sottmann
Roberto Homs-Regojo
David S. Wragg
Helmer Fjellvåg
Serena Margadonna
Hermann Emerich
format Journal article
container_title Journal of Applied Crystallography
container_volume 49
container_issue 6
container_start_page 1972
publishDate 2016
institution Swansea University
issn 1600-5767
doi_str_mv 10.1107/S160057671601428X
college_str Faculty of Science and Engineering
hierarchytype
hierarchy_top_id facultyofscienceandengineering
hierarchy_top_title Faculty of Science and Engineering
hierarchy_parent_id facultyofscienceandengineering
hierarchy_parent_title Faculty of Science and Engineering
department_str School of Engineering and Applied Sciences - Chemical Engineering{{{_:::_}}}Faculty of Science and Engineering{{{_:::_}}}School of Engineering and Applied Sciences - Chemical Engineering
url https://doi.org/10.1107/S160057671601428X
document_store_str 1
active_str 0
description A fully operational setup (electrochemical cells, sample changer and interfacing software) that enables combined quasi-simultaneous operando X-ray diffraction (XRD) and absorption (XANES and EXAFS) measurements coupled with electrochemical characterization has been realized for synchrotron based studies. Combined XRD, XANES and EXAFS analysis provides a deep insight into the working mechanisms of electrode materials.
published_date 2016-12-31T13:01:00Z
_version_ 1821954131385909248
score 11.048149

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