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Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes

Jennifer Rudd Orcid Logo, Cathren Gowenlock Orcid Logo, Virginia Gomez Orcid Logo, Ewa Kazimierska, Abdullah M. Al-Enizi, Enrico Andreoli Orcid Logo, Andrew Barron Orcid Logo

Journal of Materials Science & Technology, Volume: 35, Issue: 6, Pages: 1121 - 1127

Swansea University Authors: Jennifer Rudd Orcid Logo, Cathren Gowenlock Orcid Logo, Virginia Gomez Orcid Logo, Ewa Kazimierska, Enrico Andreoli Orcid Logo, Andrew Barron Orcid Logo

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DOI (Published version): 10.1016/j.jmst.2019.01.002

Abstract

Copper-decorated carbon nanotubes (CNTs) have important applications as precursors for ultra-conductive copper wires. Tenorite-decorated CNTs (CuO-CNTs) are ideal candidate and are currently used in laborious processes. For this reason, we have developed a facile and scalable method for the synthesi...

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Published in: Journal of Materials Science & Technology
ISSN: 10050302
Published: 2019
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URI: https://cronfa.swan.ac.uk/Record/cronfa48309
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spelling 2019-03-11T11:57:52.0238988 v2 48309 2019-01-21 Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes c2e4cf0f048a86b5ca2f331e6c566aff 0000-0002-5209-477X Jennifer Rudd Jennifer Rudd true false 3e999073c98799427c833bb5d331ef51 0000-0001-5774-5263 Cathren Gowenlock Cathren Gowenlock true false 2b0a7a13d79d306b3e0be7d30df54844 0000-0002-7846-9066 Virginia Gomez Virginia Gomez true false acd104d55246ee2d03420795510359e9 Ewa Kazimierska Ewa Kazimierska true false cbd843daab780bb55698a3daccd74df8 0000-0002-1207-2314 Enrico Andreoli Enrico Andreoli true false 92e452f20936d688d36f91c78574241d 0000-0002-2018-8288 Andrew Barron Andrew Barron true false 2019-01-21 BBU Copper-decorated carbon nanotubes (CNTs) have important applications as precursors for ultra-conductive copper wires. Tenorite-decorated CNTs (CuO-CNTs) are ideal candidate and are currently used in laborious processes. For this reason, we have developed a facile and scalable method for the synthesis of CuO-CNTs from copper acetate. It was found that the optimal loading of copper acetate onto the CNTs was 23.1 wt% and that three 1-minute microwave treatments were sufficient for the decomposition of copper acetate to copper oxide. The loading of copper oxide onto the nanotubes was confirmed using X-ray photoelectron spectroscopy, energy-dispersive X-ray spectroscopy and thermogravimetric analysis. The materials were characterised using X-ray diffraction and scanning electron microscopy. Journal Article Journal of Materials Science & Technology 35 6 1121 1127 10050302 microwave-assisted synthesis, multi-walled carbon nanotubes, tenorite, nanoparticle 30 6 2019 2019-06-30 10.1016/j.jmst.2019.01.002 COLLEGE NANME Business COLLEGE CODE BBU Swansea University 2019-03-11T11:57:52.0238988 2019-01-21T13:16:13.7509760 Faculty of Science and Engineering School of Engineering and Applied Sciences - Uncategorised Jennifer Rudd 0000-0002-5209-477X 1 Cathren Gowenlock 0000-0001-5774-5263 2 Virginia Gomez 0000-0002-7846-9066 3 Ewa Kazimierska 4 Abdullah M. Al-Enizi 5 Enrico Andreoli 0000-0002-1207-2314 6 Andrew Barron 0000-0002-2018-8288 7 0048309-21012019131924.pdf rudd2019.pdf 2019-01-21T13:19:24.1200000 Output 14626049 application/pdf Accepted Manuscript true 2020-01-11T00:00:00.0000000 true eng
title Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes
spellingShingle Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes
Jennifer Rudd
Cathren Gowenlock
Virginia Gomez
Ewa Kazimierska
Enrico Andreoli
Andrew Barron
title_short Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes
title_full Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes
title_fullStr Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes
title_full_unstemmed Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes
title_sort Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes
author_id_str_mv c2e4cf0f048a86b5ca2f331e6c566aff
3e999073c98799427c833bb5d331ef51
2b0a7a13d79d306b3e0be7d30df54844
acd104d55246ee2d03420795510359e9
cbd843daab780bb55698a3daccd74df8
92e452f20936d688d36f91c78574241d
author_id_fullname_str_mv c2e4cf0f048a86b5ca2f331e6c566aff_***_Jennifer Rudd
3e999073c98799427c833bb5d331ef51_***_Cathren Gowenlock
2b0a7a13d79d306b3e0be7d30df54844_***_Virginia Gomez
acd104d55246ee2d03420795510359e9_***_Ewa Kazimierska
cbd843daab780bb55698a3daccd74df8_***_Enrico Andreoli
92e452f20936d688d36f91c78574241d_***_Andrew Barron
author Jennifer Rudd
Cathren Gowenlock
Virginia Gomez
Ewa Kazimierska
Enrico Andreoli
Andrew Barron
author2 Jennifer Rudd
Cathren Gowenlock
Virginia Gomez
Ewa Kazimierska
Abdullah M. Al-Enizi
Enrico Andreoli
Andrew Barron
format Journal article
container_title Journal of Materials Science & Technology
container_volume 35
container_issue 6
container_start_page 1121
publishDate 2019
institution Swansea University
issn 10050302
doi_str_mv 10.1016/j.jmst.2019.01.002
college_str Faculty of Science and Engineering
hierarchytype
hierarchy_top_id facultyofscienceandengineering
hierarchy_top_title Faculty of Science and Engineering
hierarchy_parent_id facultyofscienceandengineering
hierarchy_parent_title Faculty of Science and Engineering
department_str School of Engineering and Applied Sciences - Uncategorised{{{_:::_}}}Faculty of Science and Engineering{{{_:::_}}}School of Engineering and Applied Sciences - Uncategorised
document_store_str 1
active_str 0
description Copper-decorated carbon nanotubes (CNTs) have important applications as precursors for ultra-conductive copper wires. Tenorite-decorated CNTs (CuO-CNTs) are ideal candidate and are currently used in laborious processes. For this reason, we have developed a facile and scalable method for the synthesis of CuO-CNTs from copper acetate. It was found that the optimal loading of copper acetate onto the CNTs was 23.1 wt% and that three 1-minute microwave treatments were sufficient for the decomposition of copper acetate to copper oxide. The loading of copper oxide onto the nanotubes was confirmed using X-ray photoelectron spectroscopy, energy-dispersive X-ray spectroscopy and thermogravimetric analysis. The materials were characterised using X-ray diffraction and scanning electron microscopy.
published_date 2019-06-30T03:58:42Z
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score 10.999161

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